NMR and MRI Instruments
NMR-1 Varian UnityPlus 300 (located in 147 SCH) Magnet: Oxford long hold 7.05 T, narrow bore 51 mm, 13 room temperature shims Console: two rf channels covering frequency ranges 12-309.5 MHz, 299.5-300.5 MHz Host computer: Sun Ultra 30, Solaris 7 NMR Software: VNMR 6.1C Probe: 5 mm, 4 nucleus switchable 1H/19F/31P/13C, VT compatible -100 to +150 oC Additional accessory: SMS autosampler (Zymark) with a maximum capacity of 50 samples Plotter/Printer: HP LaserJet 2200D |
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NMR-2 Varian UnityPlus 300 (located in 147 SCH) Magnet: Oxford long hold 7.05 T, narrow bore 51 mm, 13 room temperature shims Console: two rf channels covering frequency ranges 12-309.5 MHz, 299.5-300.5 MHz Host computer: Sun Ultra 30, Solaris 8 NMR Software: VNMR 6.1C Probes: a) 5 mm broadband 15N-31P, 1H or 19F decoupling b) 10 mm broadband 15N-31P, 1H decoupling, without 11B background signal c) 10 mm broadband low frequency 14-31 MHz 39K-15N, 1H decoupling All probes are VT compatible -100 to +150 oC Plotter/Printer: HP LaserJet 4 |
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Bruker AVANCE DPX 400 (located in 147 SCH) Magnet: Bruker actively shielded 9.39 T, narrow bore 54 mm, 20 room temperature shims Console: two rf channels covering frequency ranges 1H-19F and 6-242 MHz, respectively, with the capability of selective excitation, pulsed field gradient (PFG) module GRASP II/A, HR MAS accessory Host computer: HP xw4200, RHEL 4 NMR Software: TopSpin 1.3, pl 6 Probes: a) Nalorac 5 mm broadband 15N-31P, 1H or 19F decoupling, without 11B background signal, Z-PFG 100 G/cm, VT compatible -80 to +130 oC b) Nalorac 5 mm ID 1H-19F/15N-31P, Z-PFG 100 G/cm, VT compatible -80 to +130 oC c) Bruker 4 mm HR MAS 1H/13C, Z-PFG 45 G/cm, VT compatible -20 to +70 oC Plotter/Printer: HP LaserJet 4050 |
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Bruker AVANCE III 400 (located in 118 Jordan Hall) Magnet: Bruker UltraShield Plus 9.39 T, narrow bore 54 mm, BOSS-1 20 shim system, BSMS shim and digital lock control units Console: two rf channels, BLA2BB broadband amplifier system, PFG module GRASP II, BVT-3200 VT control unit, automatic tuning and matching accessory Host computer: HP xw4300, Windows XP SP2 NMR Software: TopSpin 2.0, pl 5 Probes: a) 5 mm broadband (BBFO) 15N-31P and 19F observe, 1H decoupling, Z-axis PFG, VT compatible -80 to +130 oC Additional accessory: B-ACS automatic sample changer with a maximum capacity of 120 samples Plotter/Printer: Cannon Jet Printer |
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Varian INOVA-500 (located in 136A NSH) Magnet: Oxford 11.74 T, narrow bore 51 mm, 28 room temperature shims Console: four rf channels: frequency ranges 499.5-500.5 MHz, 20-600 MHz, 20-300 MHz, and 20-300 MHz, respectively, all channels are equipped with waveform generators, PFG module Performa XYZ, deuterium automation module Host computer: Sun Ultra 30, Solaris 8 NMR Software: VNMR 6.1C Probes: a) 5 mm broadband 15N-31P, 1H decoupling b) 5 mm triple resonance 1H/13C/15N, X/Y/Z-axis PFG, VT compatible 0 to +50 oC c) 5 mm dual 1H/19F d) 5 mm inverse detection 1H-19F/15N-31P e) 10 mm broadband 15N-31P, 1H decoupling f) 16 mm broadband 15N-31P, 1H decoupling The probes a), c) - f) are VT compatible -100 to +150 oC Plotter/Printer: HP-LaserJet 4000T |
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Varian DirectDrive 600 (located in 142 NSH) Magnet: Oxford 14.09 T, narrow bore 51 mm, 28 room temperature shims Console: three rf channels: Direct Drive architecture, complete waveform shaping capability, channel 1 high band (1H/19F), channels 2 and 3 low band (20-245 MHz), PFG module Performa IV, automatic tuning and matching accessory, Host computer: Dell Precision 390N, RHEL 4 NMR Software: VNMRJ 2.2C Probes: a) 5 mm 1H-19F/15N - 31P AutoX dual broadband, Z-axis PFG, VT compatible -80 to +130 oC b) 5 mm 1H/13C/15N-31P tunable triple resonance, Z-axis PFG, VT compatible -100 to +130 oC c) Nalorac 3 mm 1H / 13C dual, VT compatible -100 to +150 oC Plotter / Printer: HP LaserJet 2200D |
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Bruker AVANCE 700 (located in 164 Stepan Addition) Magnet: Bruker UltraShield 16.45 T, 54 mm bore, BOSS-2 34 shim system, BSMS shim and digital lock control units Console: four rf channels, linear amplifier BLAXH 500/100, two linear broadband amplifiers BLAX 500, PFG module GRASP III, BVT-3000 VT control unit with BCU-5 pre-cooling accessory Host Computer: HP xw4100, RHEL 3 NMR Software: TopSpin 1.3, pl 4 Probes: a) 5 mm inverse triple resonance (TCI) 1H/13C/15N, Z-axis PFG, VT compatible 0 to +60 oC b) 5 mm inverse triple resonance (TXI) 1H/13C/15N, Z-axis PFG, VT compatible -50 to +80 oC Plotter / Printer: HP LaserJet 1300 |
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Bruker AVANCE II 800 (located in 164 Stepan Addition) Magnet: Bruker UltraStabilized and UltraShield 18.79 T, 54 mm bore, BOSS-2 34 shim system, BSMS shim and digital lock control units Console: four rf channels, linear amplifier BLAXH 500/100, two linear broadband amplifiers BLAX 500, PFG module GRASP III, BVT-3000 VT control unit with BCU-5 pre-cooling accessory, automatic tuning and matching accessory Host Computer: HP xw4200, RHEL 4 NMR Software: TopSpin 2.0, pl 5 Probes: a) 5 mm inverse triple resonance (TCI) 1H/13C/15N, Z-axis PFG, VT compatible 0 to +60 oC b) 5 mm inverse triple resonance (TXI) 1H/13C/15N, Z-axis PFG, VT compatible -50 to +80 oC c) 5 mm broadband (BBO) 15N-31P, 1H decoupling, Z-axis PFG, VT compatible -150 to +150 oC Plotter / Printer: HP color LaserJet 2550n, HP LaserJet 1320 |
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Bruker MRI DRX 300 (located in 102B NSH) Magnet: Bruker 7.05 T, superwide bore 150 mm, 13 or 20 room temperature shims depending on gradient coil used Console: two RF channels covering frequency ranges 1H-19F and 6-242 MHz, respectively. Host computer: HP xw4100, RHEL 3 NMR Software: ParaVision 3.0.2, XwinNMR 3.5 pl 6 Probe: a) Micro 2.5 gradient coil producing up to 100 Gauss/cm with 2.5 mm, 5 mm, 10 mm, 15 mm, 20 mm, 25 mm, 30 mm, 35 mm 1H RF coils, VT compatible -50 to +100 oC. b) Mini 0.36 gradient producing up to coil 14 Gauss/cm with 60 mm 1H RF coil. Additional accessory: CardioGuard, providing respiratory and cardiac gating; FTS 40 air cooling unit. Plotter/Printer: HP LaserJet 4050 |
Workstations
Spin: HP xw4300, RHEL 4; NMR software TopSpin 2.0, pl 5 and VNMRJ 2.2C, located in 136A NSH
Bloch: SunBlade 1000, Solaris 8; NMR software VNMR 6.1C, located in 147 SCH
Inova5: Sun UltraSparc 10, Solaris 8; NMR software VNMR 6.1C, located in 136A NSH